ROUTINE DATA GENERATION FOR SUGAR MILL AND REFINERY APPLICATIONS USING A LABORATORY-BASED NEAR INFRARED (NIR) INSTRUMENT
By DAVID A DONALD; BEN G GRAHAM; STEPHEN P STAUNTON; JOEL M SIMPSON; MICHAEL G O’SHEA
THE ROUTINE OPERATION of sugar mills and refineries is heavily dependent upon the
generation of laboratory data for various factory substrates. Many laboratory methods
are technically demanding, costly, time-consuming and require dedicated laboratories
and equipment. Near infrared (NIR) analyses provide a number of advantages over
other methods including reduced labour and consumable costs, enhanced throughput,
non-destructive sample preparation and analysis. This paper describes the development
of NIR-based calibrations for a wide range of sugar mill and refinery process steams
which can be used on laboratory-based NIR instruments. These instruments can be
located and operated in sugar mill and refinery laboratories with a minimum of staff
training and dedicated expertise required. Calibration sets have been developed for the
analysis of raw/refined/liquid sugars, liquors, high/low grade syrups, magma, molasses,
massecuite, mill mud, raw wash, scum, juice and bagasse, covering applications within
sugar mill and/or refinery process streams. Laboratory NIR systems can provide a very
cost effective means of delivering routine analytical data and subsequent process
decisions or applications from relatively simple easy-to-use instruments.